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Journal Articles

Principal preferred orientation evaluation of steel materials using time-of-flight neutron diffraction

Xu, P. G.; Zhang, S.-Y.*; Harjo, S.; Vogel, S. C.*; Tomota, Yo*

Quantum Beam Science (Internet), 8(1), p.7_1 - 7_13, 2024/01

Journal Articles

Validation of the applicability of the best-fit fatigue curves for 550$$^{circ}$$C in Mod.9Cr-1Mo steel to 1$$times$$10$$^{11}$$ cycles

Toyota, Kodai; Imagawa, Yuya; Onizawa, Takashi; Kato, Shoichi; Furuya, Yoshiyuki*

Nihon Kikai Gakkai Rombunshu (Internet), 89(928), p.23-00206_1 - 23-00206_15, 2023/12

In order to design fast reactors, it is necessary to consider high cycle fatigue of structural materials up to 1$$times$$10$$^{9}$$ cycles; to evaluate high cycle fatigue at 1$$times$$10$$^{9}$$ cycles, it is necessary to develop a best-fit fatigue curve applicable up to 1$$times$$10$$^{11}$$ cycles. In this study, high cycle fatigue tests were conducted under strain-controlled conditions and ultrasonic fatigue tests were also conducted to develop a high cycle fatigue evaluation method for Mod.9Cr-1Mo steel, which is a candidate material for fast reactor structural materials. Based on the test results, the best-fit fatigue curves were extended and the applicability of the JSME best-fit fatigue curves up to 1$$times$$10$$^{11}$$ cycles was verified.

Journal Articles

Cryogenic impact fracture behavior of a high-Mn austenitic steel using electron backscatter diffraction and neutron Bragg-edge transmission imaging

Wang, Y. W.*; Wang, H. H.*; Su, Y. H.; Xu, P. G.; Shinohara, Takenao

Materials Science & Engineering A, 887, p.145768_1 - 145768_13, 2023/11

 Times Cited Count:1 Percentile:54.26(Nanoscience & Nanotechnology)

Journal Articles

Numerical interpretation of thermal desorption spectra of hydrogen from high-carbon ferrite-austenite dual-phase steel

Ebihara, Kenichi; Sekine, Daiki*; Sakiyama, Yuji*; Takahashi, Jun*; Takai, Kenichi*; Omura, Tomohiko*

International Journal of Hydrogen Energy, 48(79), p.30949 - 30962, 2023/09

 Times Cited Count:0 Percentile:0.01(Chemistry, Physical)

To understand hydrogen embrittlement (HE), which is one of the stress corrosion cracking of steel materials, it is necessary to know the H distribution in steel, which can be effectively interpreted by numerical simulation of thermal desorption spectra. In weld metals and TRIP steels, residual austenite significantly influences the spectra, but a clear H distribution is not well known. In this study, an originally coded two-dimensional model was used to numerically simulate the previously reported spectra of high-carbon ferritic-austenitic duplex stainless steels, and it was found that H is mainly trapped at the carbide surface when the amount of H in the steel is low and at the duplex interface when the amount of H is high. It was also found that the thickness dependence of the H desorption peak for the interface trap site is caused by a different reason than the conventional one.

Journal Articles

Study on eutectic melting behavior of control rod materials in core disruptive accidents of sodium-cooled fast reactors; Project overview and progress until JFY2022

Yamano, Hidemasa; Takai, Toshihide; Emura, Yuki; Fukuyama, Hiroyuki*; Nishi, Tsuyoshi*; Morita, Koji*; Nakamura, Kinya*; Pellegrini, M.*

Nihon Kikai Gakkai 2023-Nendo Nenji Taikai Koen Rombunshu (Internet), 5 Pages, 2023/09

A research project has been conducting thermophysical property measurement of a eutectic melt, eutectic melting reaction and relocation experiments, eutectic reaction mechanism investigation, and physical model development on the eutectic melting reaction for reactor application analysis in order to simulate the eutectic melting reaction and relocation behavior of boron carbide as a control rod material and stainless steel during a core disruptive accident in an advanced sodium-cooled fast reactor designed in Japan. This paper describes the project overview and progress until JFY2022.

Journal Articles

Corrosion fatigue crack growth behavior of a structurally gradient steel for high-speed railway axles

Ao, N.*; Zhang, H.*; Xu, H. H.*; Wu, S. C.*; Liu, D.*; Xu, P. G.; Su, Y. H.; Kang, Q. H.*; Kang, G. Z.*

Engineering Fracture Mechanics, 281, p.109166_1 - 109166_14, 2023/03

 Times Cited Count:5 Percentile:85.05(Mechanics)

Journal Articles

High-temperature creep properties of 9Cr-ODS tempered martensitic steel and quantitative correlation with its nanometer-scale structure

Otsuka, Satoshi; Shizukawa, Yuta; Tanno, Takashi; Imagawa, Yuya; Hashidate, Ryuta; Yano, Yasuhide; Onizawa, Takashi; Kaito, Takeji; Onuma, Masato*; Mitsuhara, Masatoshi*; et al.

Journal of Nuclear Science and Technology, 60(3), p.288 - 298, 2023/03

 Times Cited Count:4 Percentile:78.52(Nuclear Science & Technology)

JAEA has been developing 9Cr-oxide dispersion strengthened (ODS) tempered martensitic steel(TMS) as a candidate material for the fuel cladding tubes of sodium-cooled fast reactors(SFRs). The reliable prediction of in-reactor creep-rupture strength is critical for implementing the 9Cr-ODS TMS cladding tube in the SFR. This study investigated the quantitative correlation between the creep properties of 9Cr-ODS TMS at 700 $$^{circ}$$C and the dispersions of nanosized oxides by analyzing the creep data and the material's nanostructure. The possibility of deriving a formula for estimating the in-reactor creep properties of 9Cr-ODS TMSs based on an analysis of the nanostructure of neutron-irradiated 9Cr-ODS TMSs was also discussed. The creep properties of 9Cr-ODS TMS at 700 $$^{circ}$$C closely correlated with the dispersion of nanosized oxide particles. The correlation between creep-rupture lives and nanosized oxide particle dispersion was determined using existing creep models. The elucidation of correlation between the stress exponent of secondary creep rate and the nanostructure is essential to enhance future modeling reliability and formulation.

Journal Articles

Defect analysis of matrix damage in reactor pressure vessel steel using WB-STEM

Yoshida, Kenta*; Toyama, Takeshi*; Inoue, Koji*; Nagai, Yasuyoshi*; Shimodaira, Masaki

Materia, 62(3), p.154 - 158, 2023/03

no abstracts in English

Journal Articles

Raman spectroscopy of eutectic melting between boride granule and stainless steel for sodium-cooled fast reactors

Fukai, Hirofumi*; Furuya, Masahiro*; Yamano, Hidemasa

Nuclear Engineering and Technology, 55(3), p.902 - 907, 2023/03

 Times Cited Count:1 Percentile:0.01(Nuclear Science & Technology)

This paper addresses reaction products and their distribution of the eutectic melting/solidifying reaction of boron carbide (B$$_{4}$$C) and stainless-steel (SS). The influence of the existence of carbon on the B$$_{4}$$C-SS eutectic reaction was investigated by comparing the iron boride (FeB)-SS reaction by Raman spectroscopy with Multivariate Curve Resolution (MCR) analysis. The scanning electron microscopy with dispersive X-ray spectrometer was also used to investigate the elemental information of the pure metals such as Cr, Ni, and Fe. In the B$$_{4}$$C-SS samples, a new layer was formed between B$$_{4}$$C/SS interface, and the layer was confirmed that the formed layer corresponded to amorphous carbon (graphite) or FeB or Fe$$_{2}$$B. In contrast, a new layer was not clearly formed between FeB and SS interface in the FeB-SS samples.

Journal Articles

High temperature mechanical properties and microstructure in 9Cr or 12Cr oxide dispersion strengthened steels

Mitsuhara, Masatoshi*; Kurino, Koichi*; Yano, Yasuhide; Otsuka, Satoshi; Toyama, Takeshi*; Onuma, Masato*; Nakashima, Hideharu*

Tetsu To Hagane, 109(3), p.189 - 200, 2023/03

 Times Cited Count:0 Percentile:0(Metallurgy & Metallurgical Engineering)

Oxide Dispersion Strengthened (ODS) ferritic steel, a candidate material for fast reactor fuel cladding, has low thermal expansion, good thermal conductivity, and excellent resistance to irradiation damage and high temperature strength. The origin of the excellent high-temperature strength lies in the dispersion of fine oxides. In this study, creep tests at 700 or 750$$^{circ}$$C, which are close to the operating temperatures of fast reactors, and high-temperature tensile tests at 900 to 1350 $$^{circ}$$C, which simulate accident conditions, were conducted on 9Cr ODS ferritic steels, M11 and MP23, and 12Cr ODS ferritic steel, F14, to confirm the growth behavior of oxides. In the M11 and F14 creep test samples, there was little oxide growth or decrease in number density from the initial state, indicating that dispersion strengthening by oxides was effective during deformation. After creep deformation of F14, the development of dislocation substructures such as dislocation walls and subgrain boundaries was hardly observed, and mobile dislocations were homogeneously distributed in the grains. The dislocation density increased with increasing stress during the creep test. In the high-temperature ring tensile tests of MP23 and F14, the strength of both steels decreased at higher temperatures. In MP23, elongation decreased with increasing test temperature from 900 to 1100 $$^{circ}$$C, but increased at 1200 $$^{circ}$$C, decreased drastically at 1250 $$^{circ}$$C, and increased again at 1300 $$^{circ}$$C. In F14, elongation decreased with increasing temperature. It was inferred that the formation of the $$delta$$-ferrite phase was responsible for this complex change in mechanical properties of MP23 from 1200 to 1300 $$^{circ}$$C.

Journal Articles

Fatigue crack non-propagation behavior of a gradient steel structure from induction hardened railway axles

Zhang, H.*; Wu, S. C.*; Ao, N.*; Zhang, J. W.*; Li, H.*; Zhou, L.*; Xu, P. G.; Su, Y. H.

International Journal of Fatigue, 166, p.107296_1 - 107296_11, 2023/01

 Times Cited Count:4 Percentile:61.91(Engineering, Mechanical)

Journal Articles

Effect of nitrogen concentration on creep strength and microstructure of 9Cr-ODS ferritic/martensitic steel

Oka, Hiroshi*; Tanno, Takashi; Yano, Yasuhide; Otsuka, Satoshi; Kaito, Takeji; Hashimoto, Naoyuki*

Journal of Nuclear Materials, 572, p.154032_1 - 154032_8, 2022/12

 Times Cited Count:3 Percentile:68.71(Materials Science, Multidisciplinary)

9Cr oxide dispersion strengthened steels with slightly different nitrogen concentrations (0.0034 - 0.029 wt%) were prepared and their creep property at 973 K was investigated with microstructural characterization before and after the creep test. The creep strength decreased significantly as the nitrogen concentration increased. Microstructural observation revealed that, in the higher nitrogen concentration specimen, coarse Y-rich inclusions were found along the boundary between transformed ferrite region and residual ferrite region. The solubility difference of nitrogen in $$alpha$$ and $$gamma$$ phase would induce the localized increment of nitrogen concentration in the boundary region during the austenitizing process, resulting in the thermodynamic destabilization and subsequent coarsening of the dispersed oxide particles. The rows of creep voids were found near the rupture part of the crept specimen, suggesting that the coarse inclusions were the starting point of creep void formation and the subsequent premature fracture.

Journal Articles

Liquid decontamination using acidic electrolyzed water for various uranium-contaminated steel surfaces in dismantled centrifuge

Sakasegawa, Hideo; Nomura, Mitsuo; Sawayama, Kengo; Nakayama, Takuya; Yaita, Yumi*; Yonekawa, Hitoshi*; Kobayashi, Noboru*; Arima, Tatsumi*; Hiyama, Toshiaki*; Murata, Eiichi*

Progress in Nuclear Energy, 153, p.104396_1 - 104396_9, 2022/11

 Times Cited Count:0 Percentile:0.01(Nuclear Science & Technology)

When dismantling centrifuges in uranium-enrichment facilities, decontamination techniques must be developed to remove uranium-contaminated surfaces of dismantled parts selectively. Dismantled uranium-contaminated parts can be disposed of as nonradioactive wastes or recycled after decontamination appropriate for clearance. previously, we developed a liquid decontamination technique using acidic electrolyzed water to remove uranium-contaminated surfaces. However, further developments are still needed for its actual application. Dismantled parts have various uranium-contaminated surface features due to varied operational conditions, inhomogeneous decontamination using iodine heptafluoride gas, and changes in long-term storage conditions after dismantling. Here, we performed liquid decontamination on specimens with varying uranium-contaminated surfaces cut from a centrifuge made of low-carbon steel. From the results, the liquid decontamination can effectively remove the uranium-contaminated surfaces, and radioactive concentrations fell below the target value within twenty minutes. Although the required time should also depend on dismantled parts' sizes and shapes in their actual application, we demonstrated that it could be an effective decontamination technique for uranium-contaminated steels of dismantled centrifuges.

Journal Articles

Revisit deformation behavior of lath martensite

Harjo, S.; Gong, W.; Kawasaki, Takuro; Morooka, Satoshi; Yamashita, Takayuki*

ISIJ International, 62(10), p.1990 - 1999, 2022/10

 Times Cited Count:1 Percentile:0(Metallurgy & Metallurgical Engineering)

Journal Articles

Experimental study on reaction behavior between control rod material and molten stainless steel for core disruptive accidents of sodium-cooled fast reactors

Emura, Yuki; Kamiyama, Kenji; Yamano, Hidemasa

Dai-26-Kai Doryoku, Enerugi Gijutsu Shimpojiumu Koen Rombunshu (Internet), 4 Pages, 2022/07

no abstracts in English

Journal Articles

Failure bending stresses for small diameter thick-wall pipes

Yamaguchi, Yoshihito; Hasegawa, Kunio; Li, Y.; Lacroix, V.*

Proceedings of ASME 2022 Pressure Vessels and Piping Conference (PVP 2022) (Internet), 4 Pages, 2022/07

Journal Articles

Effects of potential on the electrical conductivity of a solution within a crevice of stainless steel in high-temperature water

Soma, Yasutaka; Komatsu, Atsushi; Ueno, Fumiyoshi

Corrosion, 78(6), p.503 - 515, 2022/06

 Times Cited Count:0 Percentile:0(Materials Science, Multidisciplinary)

The effects of electrochemical potential (ECP) on water chemistry within a crevice are of critical importance for understanding stress corrosion cracking (SCC) of Fe-Cr-Ni alloys in high temperature water. In this study, the effects of ECP on the electrical conductivity of a solution within a Type-316L stainless steel crevice ($$sigma$$$$_{crev}$$) have been studied in 288$$^{circ}$$C and 8 MPa water containing 10 ppb Cl$$^{-}$$ as major anionic species. In situ measurements of $$sigma$$$$_{crev}$$ in a rectangular crevice with a gap of 15 $$mu$$m and a depth of 23 mm have been conducted using small sensors installed at different crevice depths. An increase in ECP from -0.49 V (vs. standard hydrogen electrode) to -0.12 V resulted in an increase in $$sigma$$$$_{crev}$$ from 12 $$mu$$Scm$$^{-1}$$ to 160 $$mu$$Scm$$^{-1}$$ at a distance of 21 mm from the crevice mouth. The increase in $$sigma$$$$_{crev}$$ reached a maximum at about 0.15 V (about 300 $$mu$$Scm$$^{-1}$$) and then tended to decrease with increasing potential. Finite element model analysis taking into account the electrochemical reaction quantitatively reproduced this behavior. It is considered that Cl$$^{-}$$ is the major anionic species transported into the crevice at relatively low potentials, and that $$sigma$$$$_{crev}$$ increases monotonically with increasing ECP. On the other hand, when ECP exceeds around 0 V, a sufficient amount of HCrO$$_{4}$$$$^{-}$$ generated by transpassive dissolution also transported into the gap. Since this chemical species is highly oxidizing, unlike Cl, it is assumed that it reacts with metal cations to oxidize and precipitate them, thereby lowering conductivity.

Journal Articles

Viscosity measurements of molten metal using an improved oscillating crucible method

Sato, Rika*; Nishi, Tsuyoshi*; Ota, Hiromichi*; Yamano, Hidemasa

International Journal of Thermophysics, 43(6), p.85_1 - 85_15, 2022/06

 Times Cited Count:0 Percentile:0.01(Thermodynamics)

In this study, we developed a simple viscosity measurement method based on the principle of least squares to derive the period and logarithmic decrement of oscillation. To confirm the reproducibility of the proposed method, the viscosity of molten nickel was measured and found to be in good agreement with those reported in the literature. The measurement error was less than $$pm$$3%. Further, the experimental data showed good reproducibility, and the measurements were obtained with high accuracies using the proposed method.

Journal Articles

Viscosity measurements of Molten casting steels for high temperature using an oscillating crucible viscometer

Takatsuka, Yuriko*; Matsumoto, Saori*; Nishi, Tsuyoshi*; Ota, Hiromichi*; Hori, Ayumi*; Hayashi, Kiichiro*; Yamano, Hidemasa

Jikken Rikigaku, 22(2), p.117 - 119, 2022/06

This study clarified the effect of the viscosities of molten casting steels for high temperature by measuring them using the oscillating crucible method. The casting steels for high temperature samples used for viscosity measurements contained 0, 10, 20, 30, 40, and 50 mass% Ni. Viscosities were evaluated using Roscoe's equation and measured in the temperature range of 1693-1803 K.

Journal Articles

Leaching behavior of multiphase solidified melt prepared from stainless steel and Zircaloy

Ikeuchi, Hirotomo

Journal of Nuclear Science and Technology, 59(6), p.768 - 780, 2022/06

 Times Cited Count:1 Percentile:31.61(Nuclear Science & Technology)

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